5D23
The crystal structure of STPR from Bombyx mori in complex with 13-bp DNA derived from the +290 site of fibroin gene
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-10-21 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | H 3 2 |
Unit cell lengths | 123.180, 123.180, 73.574 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.450 - 1.950 |
R-factor | 0.20616 |
Rwork | 0.205 |
R-free | 0.23192 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.299 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.950 |
Number of reflections | 15446 |
<I/σ(I)> | 12.6 |
Completeness [%] | 98.2 |
Redundancy | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 15% PEG4000, 20% 2-propanol, 0.1M sodium citrate pH5.6 |