5CZY
Crystal structure of LegAS4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9796 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 69.249, 69.249, 200.497 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 66.832 - 2.200 |
R-factor | 0.2046 |
Rwork | 0.202 |
R-free | 0.24760 |
Starting model (for MR) | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.122 |
Data scaling software | XSCALE |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 66.832 | 2.330 | |
High resolution limit [Å] | 2.200 | 6.570 | 2.200 |
Rmerge | 0.069 | 0.041 | 0.548 |
Rmeas | 0.071 | 0.042 | 0.590 |
Total number of observations | 490905 | ||
Number of reflections | 28465 | 1233 | 4013 |
<I/σ(I)> | 29.36 | 65.78 | 3.29 |
Completeness [%] | 97.3 | 99.6 | 86.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 0.1M sodium citrate, 15 % (v/v) isopropanol, 10%(w/v) PEG 10000 |