5CVC
Structure of maize serine racemase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-12-16 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9793 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 50.992, 204.017, 211.847 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.380 - 2.090 |
| R-factor | 0.19966 |
| Rwork | 0.198 |
| R-free | 0.22868 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3hmk |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.285 |
| Phasing software | MrBUMP |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.090 |
| Number of reflections | 64417 |
| <I/σ(I)> | 17.82 |
| Completeness [%] | 98.9 |
| Redundancy | 5.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 283 |
