5CS1
The structure of the NK1 fragment of HGF/SF
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2008-02-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.971 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.387, 63.400, 57.616 |
Unit cell angles | 90.00, 94.84, 90.00 |
Refinement procedure
Resolution | 42.560 - 2.000 |
R-factor | 0.213 |
Rwork | 0.211 |
R-free | 0.25500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1nk1 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.229 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.052 | 0.303 |
Number of reflections | 26001 | |
<I/σ(I)> | 12.5 | |
Completeness [%] | 99.5 | 96.4 |
Redundancy | 3.6 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 19% PEG 4000, 200 nM Na Acetate, 150 mM Tris |