5CKT
Crystal Structure of KorA, a plasmid-encoded, global transcription regulator
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-07-13 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.933 |
| Spacegroup name | P 1 |
| Unit cell lengths | 42.580, 49.690, 52.330 |
| Unit cell angles | 98.09, 93.87, 106.01 |
Refinement procedure
| Resolution | 27.170 - 2.000 |
| R-factor | 0.1972 |
| Rwork | 0.196 |
| R-free | 0.22170 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.812 |
| Data scaling software | XDS |
| Phasing software | SOLVE |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 27.170 | 2.070 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.438 | |
| Number of reflections | 26649 | |
| <I/σ(I)> | 26.1 | 3.6 |
| Completeness [%] | 97.2 | 96.3 |
| Redundancy | 3.9 | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | PEG 4000, sodium acetate, ammonium acetate |
