5CDZ

Crystal structure of conserpin in the latent state

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	CCD
Collection date	2014-05-09
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9537
Spacegroup name	P 62
Unit cell lengths	101.679, 101.679, 62.720
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	33.282 - 1.449
R-factor	0.1581
Rwork	0.157
R-free	0.18510
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5cdx
RMSD bond length	0.012
RMSD bond angle	1.568
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	33.282
High resolution limit [Å]	1.449
Number of reflections	65513
<I/σ(I)>	17.24
Completeness [%]	99.9
Redundancy	38

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	288	0.1 M Hepes pH 8.0, 0.2 M Ammonium Acetate, 35% v/v MPD