5CDC
Crystal Structure of Israel acute Paralysis Virus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-05-29 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 343.149, 383.261, 329.911 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 70.000 - 4.000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1b35 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 70.000 |
High resolution limit [Å] | 4.000 |
Number of reflections | 262425 |
<I/σ(I)> | 1.09 |
Completeness [%] | 72.7 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.5 | 298 | 0.1M Cadmium chloride, 0.1M Naacetate pH 4.5, 15% (v/v) PEG 400 |