5BVT
Palmitate-bound pFABP5
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
| Synchrotron site | PAL/PLS |
| Beamline | 7A (6B, 6C1) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-12-06 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9793 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 29.497, 60.250, 35.732 |
| Unit cell angles | 90.00, 113.01, 90.00 |
Refinement procedure
| Resolution | 32.890 - 2.310 |
| R-factor | 0.175 |
| Rwork | 0.170 |
| R-free | 0.26912 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.623 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 4997 |
| <I/σ(I)> | 61.3 |
| Completeness [%] | 97.6 |
| Redundancy | 7.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M magnesium chloride, 0.1 M Tris (pH 8.5), 30% (w/v) PEG 4000 |
