Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-05-06 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.97890 |
| Spacegroup name | P 1 |
| Unit cell lengths | 53.032, 73.265, 77.355 |
| Unit cell angles | 96.64, 89.77, 111.16 |
Refinement procedure
| Resolution | 14.947 - 1.952 |
| R-factor | 0.2017 |
| Rwork | 0.201 |
| R-free | 0.22280 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3c9i |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.882 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 15.000 | 2.020 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.410 | |
| Number of reflections | 72716 | |
| <I/σ(I)> | 14.45 | 2.54 |
| Completeness [%] | 93.1 | 73.1 |
| Redundancy | 1.8 | 1.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 9 | 289 | 40% PEG 4000, 0.1M potassium chloride, 0.1M TAPS buffer |
