5BR3

Crystal structure of hemagglutinin of A/Taiwan/2/2013 (H6N1) in complex with LSTa

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-G
Synchrotron site	APS
Beamline	21-ID-G
Temperature [K]	80
Detector technology	CCD
Collection date	2014-10-24
Detector	RAYONIX MX-300
Wavelength(s)	0.978
Spacegroup name	P 3
Unit cell lengths	114.010, 114.010, 163.200
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	42.239 - 2.550
R-factor	0.202
Rwork	0.201
R-free	0.22820
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	PHENIX
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	42.260
High resolution limit [Å]	2.550
Number of reflections	77363
<I/σ(I)>	8.6
Completeness [%]	100.0
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9	290	0.1 M Bicine, 10% PEG 20000 and 2% 1,4-Dioxane