5B7W

Crystal structure of the YajQ-family protein XC_3703 from Xanthomonas campestris pv.campestris

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2015-10-14
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.979
Spacegroup name	P 1 21 1
Unit cell lengths	51.510, 65.470, 52.284
Unit cell angles	90.00, 92.69, 90.00

Refinement procedure

Resolution	35.821 - 2.080
R-factor	0.2476
Rwork	0.244
R-free	0.28400
RMSD bond length	0.003
RMSD bond angle	0.582
Refinement software	PHENIX ((dev_2411: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	40.830
High resolution limit [Å]	2.080
Number of reflections	20472
<I/σ(I)>	9.5
Completeness [%]	97.4
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1M Bis-Tris pH5.5, 25% w/v Polyethylene glycol 3500