5B5M
Crystal structure of the Sr-substituted LH1-RC complex from Tch. tepidum
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-04-20 |
| Detector | RAYONIX MX300HE |
| Wavelength(s) | 0.9 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 164.888, 148.946, 210.226 |
| Unit cell angles | 90.00, 108.18, 90.00 |
Refinement procedure
| Resolution | 48.182 - 3.300 |
| R-factor | 0.2732 |
| Rwork | 0.271 |
| R-free | 0.30930 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3wmm |
| RMSD bond length | 0.035 |
| RMSD bond angle | 2.261 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.182 | 3.360 |
| High resolution limit [Å] | 3.300 | 3.300 |
| Number of reflections | 142696 | |
| <I/σ(I)> | 20.4 | |
| Completeness [%] | 98.0 | |
| Redundancy | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG 3000, strontium chloride, decylphosphocholine |
