5AXB

Crystal structure of mouse SAHH complexed with noraristeromycin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron site	Photon Factory
Beamline	AR-NE3A
Temperature [K]	100
Detector technology	CCD
Collection date	2009-10-24
Detector	ADSC QUANTUM 270
Wavelength(s)	1.0
Spacegroup name	I 2 2 2
Unit cell lengths	100.442, 104.459, 176.744
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 1.650
R-factor	0.15557
Rwork	0.154
R-free	0.18085
RMSD bond length	0.014
RMSD bond angle	1.494
Refinement software	REFMAC (5.5.0110)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.680
High resolution limit [Å]	1.650	1.650
Rmerge		0.478
Number of reflections	109318
<I/σ(I)>	40.2	2.1
Completeness [%]	98.5	82.4
Redundancy	6.5	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG 3350