5AV4

Crystal structure of DAPK1-genistein complex in the presence of bromide ions.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron site	Photon Factory
Beamline	AR-NE3A
Temperature [K]	100
Detector technology	CCD
Collection date	2014-11-21
Detector	ADSC QUANTUM 270
Wavelength(s)	0.90681
Spacegroup name	P 21 21 21
Unit cell lengths	47.022, 62.053, 88.353
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.579 - 1.400
R-factor	0.1913
Rwork	0.189
R-free	0.22760
RMSD bond length	0.006
RMSD bond angle	1.052
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Refinement software	PHENIX ((phenix.refine: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	28.600
High resolution limit [Å]	1.400
Number of reflections	50233
<I/σ(I)>	24.3
Completeness [%]	96.8
Redundancy	7.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	2 M ammonium sulfate, 0.1 M MES