5AV1

Crystal structure of DAPK1 in the presence of bromide ions.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron site	Photon Factory
Beamline	AR-NE3A
Temperature [K]	100
Detector technology	CCD
Collection date	2014-11-21
Detector	ADSC QUANTUM 270
Wavelength(s)	0.91714
Spacegroup name	P 21 21 21
Unit cell lengths	46.819, 62.279, 88.449
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.568 - 1.500
R-factor	0.1874
Rwork	0.186
R-free	0.21470
RMSD bond length	0.006
RMSD bond angle	1.067
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Refinement software	PHENIX ((phenix.refine: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	28.600
High resolution limit [Å]	1.500
Number of reflections	42094
<I/σ(I)>	43.9
Completeness [%]	99.3
Redundancy	10.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	2 M ammonium sulfate, 0.1 M MES