5AUU

Crystal structure of DAPK1 in complex with luteolin.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron site	Photon Factory
Beamline	AR-NW12A
Temperature [K]	100
Detector technology	CCD
Collection date	2014-05-18
Detector	ADSC QUANTUM 210r
Wavelength(s)	1
Spacegroup name	P 21 21 21
Unit cell lengths	47.006, 62.287, 88.479
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.068 - 1.700
R-factor	0.181
Rwork	0.179
R-free	0.21620
RMSD bond length	0.006
RMSD bond angle	1.086
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	PHENIX
Refinement software	PHENIX ((phenix.refine: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	44.200
High resolution limit [Å]	1.700
Number of reflections	28155
<I/σ(I)>	24.3
Completeness [%]	96.0
Redundancy	4.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	2 M ammonium sulfate, 0.1 M MES