5AR1
Crystal structure of Cdc11 from Saccharomyces cerevisiae
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-01-17 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 187.050, 187.050, 57.960 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 34.200 - 2.850 |
| R-factor | 0.2574 |
| Rwork | 0.257 |
| R-free | 0.25880 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2qnr |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.200 |
| Data reduction software | autoPROC |
| Data scaling software | Aimless ((VERSION 0.5.14)) |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.10.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 162.000 | 3.000 |
| High resolution limit [Å] | 2.850 | 2.850 |
| Rmerge | 0.103 | 1.052 |
| Number of reflections | 14458 | |
| <I/σ(I)> | 21.5 | 1 |
| Completeness [%] | 99.9 | 99.2 |
| Redundancy | 34.1 | 13.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | PH 5.5 |
