5ANZ

Crystal Structure of SltB3 from Pseudomonas aeruginosa.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 2M, KETEK FLUORESCENCE DETECTOR
Spacegroup name	P 21 21 2
Unit cell lengths	112.281, 61.840, 50.630
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	54.168 - 1.614
R-factor	0.1801
Rwork	0.179
R-free	0.20360
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	BALBES
RMSD bond length	0.006
RMSD bond angle	0.974
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	MOLREP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	56.140	1.700
High resolution limit [Å]	1.610	1.610
Rmerge	0.030	0.710
Number of reflections	46193
<I/σ(I)>	48.6	2.7
Completeness [%]	100.0	100
Redundancy	6.8	9.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1