5AMS
Crystal structure of Sqt1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 165.999, 165.999, 95.351 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 36.370 - 3.350 |
| R-factor | 0.1738 |
| Rwork | 0.171 |
| R-free | 0.22210 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.420 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.900 | 3.620 |
| High resolution limit [Å] | 3.350 | 3.350 |
| Rmerge | 0.050 | 0.290 |
| Number of reflections | 22101 | |
| <I/σ(I)> | 9.1 | 2 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 9.4 | 9.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
