5ALD
ligand complex structure of soluble epoxide hydrolase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E+ |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | RIGAKU A200 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 92.376, 92.376, 244.083 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 80.000 - 2.260 |
| R-factor | 0.182 |
| Rwork | 0.180 |
| R-free | 0.22700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5ahx |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.220 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | BUSTER (2.11.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 244.080 | 2.380 |
| High resolution limit [Å] | 2.260 | 2.260 |
| Rmerge | 0.160 | 1.050 |
| Number of reflections | 29929 | |
| <I/σ(I)> | 19.4 | 2.9 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 11.4 | 11.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
