5AIO

Crystal structure of t131 N-terminal TPR array

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2)
Synchrotron site	PETRA III, EMBL c/o DESY
Beamline	P14 (MX2)
Temperature [K]	100
Spacegroup name	P 62
Unit cell lengths	116.360, 116.360, 95.980
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.612 - 3.148
R-factor	0.2519
Rwork	0.250
R-free	0.28660
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.004
RMSD bond angle	0.713
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.230
High resolution limit [Å]	3.150	3.150
Rmerge	0.070
Number of reflections	12884
Completeness [%]	99.9	99.9
Redundancy	39.3	38.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1				0.2 M MGCL2, 0.1 M TRIS PH 8.3 AND 42.5% ETHYLENE GLYCOL