5AG8
CRYSTAL STRUCTURE OF A MUTANT (665I6H) OF THE C-TERMINAL DOMAIN OF RGPB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.470, 61.740, 55.300 |
Unit cell angles | 90.00, 117.79, 90.00 |
Refinement procedure
Resolution | 48.920 - 1.900 |
R-factor | 0.16227 |
Rwork | 0.161 |
R-free | 0.20247 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1cvr |
RMSD bond length | 0.019 |
RMSD bond angle | 1.980 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.920 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.050 | 0.270 |
Number of reflections | 23941 | |
<I/σ(I)> | 20.5 | 4.5 |
Completeness [%] | 98.6 | 91.9 |
Redundancy | 3.6 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 30% PEG 4000, 0.2M (NH4)2SO4, 10% PEG 300 |