5AFR
N-terminal fragment of dynein heavy chain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Collection date | 2014-05-24 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 71.899, 148.861, 179.620 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 114.620 - 5.000 |
| R-factor | 0.39488 |
| Rwork | 0.393 |
| R-free | 0.43658 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.307 |
| Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 52.600 |
| High resolution limit [Å] | 5.000 |
| Rmerge | 0.080 |
| Number of reflections | 8866 |
| <I/σ(I)> | 15.8 |
| Completeness [%] | 100.0 |
| Redundancy | 11.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
