5AFN

alpha7-AChBP in complex with lobeline and fragment 5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	CCD
Collection date	2012-11-30
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	85.520, 112.504, 143.109
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.895 - 2.149
R-factor	0.1699
Rwork	0.167
R-free	0.22310
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.007
RMSD bond angle	1.139
Refinement software	PHENIX ((PHENIX.REFINE: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	47.120
High resolution limit [Å]	2.220
Rmerge	0.090
Number of reflections	70473
<I/σ(I)>	14.3
Completeness [%]	99.9
Redundancy	7.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1