5ACJ
X-ray Structure of LPMO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 125.440, 125.440, 125.440 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.700 |
R-factor | 0.19466 |
Rwork | 0.193 |
R-free | 0.22688 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4eir |
RMSD bond length | 0.016 |
RMSD bond angle | 1.759 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.750 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.060 | 0.440 |
Number of reflections | 35016 | |
<I/σ(I)> | 36.67 | 6.16 |
Completeness [%] | 93.4 | 98.1 |
Redundancy | 34.6 | 19.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 3.0M SODIUM CHLORIDE, 100MM CITRIC ACID PH3.5, pH 5.5 |