5A9X

Structure of GDP bound BipA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-03-08
Detector	DECTRIS PILATUS 6M
Spacegroup name	I 41 3 2
Unit cell lengths	241.946, 241.946, 241.946
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.450 - 3.800
R-factor	0.25426
Rwork	0.248
R-free	0.31268
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.010
RMSD bond angle	1.521
Data reduction software	XDS
Data scaling software	XDS
Refinement software	REFMAC (5.8.0107)

Data quality characteristics

	Overall
Low resolution limit [Å]	47.450
High resolution limit [Å]	3.800
Rmerge	0.170
Number of reflections	10596
<I/σ(I)>	14.96
Completeness [%]	99.6
Redundancy	17.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1				20% (W/V) PEG3350, 0.2 M SODIUM FLUORIDE