5A98

Crystal structure of Trichoplusia ni CPV15 polyhedra

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	I 2 3
Unit cell lengths	102.890, 102.890, 102.890
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.005 - 1.816
R-factor	0.1646
Rwork	0.162
R-free	0.21990
Structure solution method	SIRAS
Starting model (for MR)	NONE
RMSD bond length	0.007
RMSD bond angle	1.276
Data reduction software	xia2
Data scaling software	xia2
Phasing software	SHARP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	51.400	1.860
High resolution limit [Å]	1.820	1.820
Rmerge	0.470
Number of reflections	16418
<I/σ(I)>	4.2	0.8
Completeness [%]	99.7	97.9
Redundancy	7.8	4.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		PH 7.5