5A96

Crystal structure of Lymantria dispar CPV14 polyhedra

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS
Spacegroup name	I 2 3
Unit cell lengths	102.600, 102.600, 102.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	32.445 - 1.914
R-factor	0.1369
Rwork	0.133
R-free	0.19400
Structure solution method	SIRAS
Starting model (for MR)	NONE
RMSD bond length	0.008
RMSD bond angle	1.225
Data reduction software	xia2
Data scaling software	xia2
Phasing software	SHARP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	72.500	2.020
High resolution limit [Å]	1.910	1.910
Rmerge	0.200	0.330
Number of reflections	12952
<I/σ(I)>	8.4	1.8
Completeness [%]	92.3	52.1
Redundancy	7.9	1.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		pH 7.5