5A8V
Crystal structure of Orgyia pseudotsugata CPV5 polyhedra with SeMet substitution
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 102.054, 102.054, 102.054 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.082 - 2.074 |
| R-factor | 0.1718 |
| Rwork | 0.169 |
| R-free | 0.22790 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.015 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | SHARP |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.200 | 2.140 |
| High resolution limit [Å] | 2.070 | 2.070 |
| Rmerge | 0.160 | 0.390 |
| Number of reflections | 10902 | |
| <I/σ(I)> | 7.5 | 1.9 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 64.1 | 26.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.5 |
