5A8U

Crystal structure of Orgyia pseudotsugata CPV5 polyhedra

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	I 2 3
Unit cell lengths	102.320, 102.320, 102.320
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	51.160 - 1.609
R-factor	0.161
Rwork	0.159
R-free	0.19670
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5a8v
RMSD bond length	0.008
RMSD bond angle	1.190
Data reduction software	xia2
Data scaling software	xia2
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	51.200	1.650
High resolution limit [Å]	1.610	1.610
Rmerge	0.340
Number of reflections	23283
<I/σ(I)>	7	1.4
Completeness [%]	100.0	100
Redundancy	14.8	10.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		pH 7.5