5A8T
Crystal structure of Antheraea mylitta CPV4 polyhedra type 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | I 2 3 |
Unit cell lengths | 104.813, 104.813, 104.813 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.012 - 2.003 |
R-factor | 0.1776 |
Rwork | 0.175 |
R-free | 0.23850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a8s |
RMSD bond length | 0.006 |
RMSD bond angle | 0.982 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.000 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.180 | 0.330 |
Number of reflections | 11543 | |
<I/σ(I)> | 8.1 | 1.7 |
Completeness [%] | 88.5 | 42.7 |
Redundancy | 7.6 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |