5A2V

Crystal structure of mtPAP in Apo form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	287
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 21 21 21
Unit cell lengths	59.391, 94.367, 191.849
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.000 - 1.820
R-factor	0.22328
Rwork	0.222
R-free	0.24532
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	NONE
RMSD bond length	0.005
RMSD bond angle	0.916
Phasing software	MOLREP
Refinement software	REFMAC (5.7.0032)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	1.920
High resolution limit [Å]	1.820	1.820
Rmerge	0.110	2.040
Number of reflections	97579
<I/σ(I)>	17	1.3
Completeness [%]	100.0	100
Redundancy	13.2	13
CC(1/2)	0.990	0.540

Crystallization Conditions

crystal ID	method	pH	temperature	details
1