5A0O
adhiron raised against p300
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-02-04 |
| Detector | DECTRIS PILATUS |
| Spacegroup name | I 21 21 21 |
| Unit cell lengths | 69.290, 72.640, 107.930 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.730 - 2.730 |
| R-factor | 0.24058 |
| Rwork | 0.239 |
| R-free | 0.27811 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4n6u |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.725 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | BALBES |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 36.730 | 2.800 |
| High resolution limit [Å] | 2.730 | 2.730 |
| Rmerge | 0.150 | 1.440 |
| Number of reflections | 7134 | |
| <I/σ(I)> | 12.3 | 1.7 |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 12.6 | 13.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 0.8 M DI-SODIUM SUCCINATE PH7 |
