5A0F
Crystal structure of Yersinia Afp18-modified RhoA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-02-21 |
Detector | RIGAKU CCD |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 91.392, 91.392, 56.628 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 91.390 - 2.000 |
R-factor | 0.20571 |
Rwork | 0.205 |
R-free | 0.21292 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dpf |
RMSD bond length | 0.013 |
RMSD bond angle | 1.671 |
Data reduction software | HKL-3000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.110 | 0.320 |
Number of reflections | 31941 | |
<I/σ(I)> | 21.3 | 5.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.8 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.1 M SODIUM ACETATE, PH 5 AND 1.5 M AMMONIUM SULFATE; SITTING-DROP VAPOR-DIFFUSION AT 293.15 K |