4V2S
Crystal structure of Hfq in complex with the sRNA RydC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-05-28 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.940, 73.356, 137.947 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.320 - 3.480 |
R-factor | 0.21989 |
Rwork | 0.217 |
R-free | 0.28158 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rer |
RMSD bond length | 0.010 |
RMSD bond angle | 1.475 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.470 | 3.690 |
High resolution limit [Å] | 3.480 | 3.480 |
Rmerge | 0.150 | 0.890 |
Number of reflections | 9190 | |
<I/σ(I)> | 9.6 | 2.3 |
Completeness [%] | 99.1 | 99.4 |
Redundancy | 5.8 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.2 M TRI-SODIUM CITRATE, 0.1 M SODIUM CACODYLATE (PH 6.5), 15% ISOPROPANOL |