4L3J

Crystal structures of human p70S6K1 kinase domain

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2011-06-20
Detector	CCD ADSC unsupported-q315
Wavelength(s)	1
Spacegroup name	P 41 21 2
格子定数 [Å]	70.511, 70.511, 150.484
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	50.000 - 2.100
R因子	0.2125
Rwork	0.210
R-free	0.25460
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3a62
結合長の平均二乗偏差(RMSD) [Å]	0.016
結合角の平均二乗偏差(RMSD) [度]	1.333
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.5.0102)

Quality characteristics

	Overall
分解能 [Å] (低)	50.000
分解能 [Å] (高)	2.100
独立反射数	22617

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1