Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4L3B

X-ray structure of the HRV2 A particle uncoating intermediate

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2012-05-04
DetectorPSI PILATUS 6M
Wavelength(s)1
Spacegroup nameI 2 2 2
Unit cell lengths311.930, 357.830, 386.670
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution121.390 - 6.500
R-factor0.309
Rwork0.309
R-free0.32000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3tn9
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareDM
Refinement softwareREFMAC (5.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]262.6304.740
High resolution limit [Å]4.5004.500
Rmerge0.163
Number of reflections15750
<I/σ(I)>4.4
Completeness [%]12.512.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52930.5 M ammonium sulfate, 1 M sodium/potassium phosphate, 5% glycerol, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K

225158

数据于2024-09-18公开中

PDB statisticsPDBj update infoContact PDBjnumon