4CWS
Human HSP90 alpha N-terminal domain in complex with an Aminotriazoloquinazoline inhibitor
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-04-15 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | I 2 2 2 |
格子定数 [Å] | 67.143, 91.529, 99.432 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 30.000 - 2.300 |
R因子 | 0.20602 |
Rwork | 0.203 |
R-free | 0.26394 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
結合長の平均二乗偏差(RMSD) [Å] | 0.013 |
結合角の平均二乗偏差(RMSD) [度] | 1.741 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.6.0117) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 2.380 |
分解能 [Å] (高) | 2.300 | 2.300 |
Rmerge_l_obs | 0.050 | 0.270 |
独立反射数 | 12942 | |
<I/σ(I)> | 17.1 | 5.8 |
完全性 [%] | 93.6 | 95.5 |
冗長性 | 5.7 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 |