4ZP9
Coxsackievirus B3 Polymerase - F364I mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-31 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.00 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 74.386, 74.386, 288.252 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.599 - 1.799 |
R-factor | 0.1972 |
Rwork | 0.196 |
R-free | 0.23320 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.825 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 52.599 | 1.910 | |
High resolution limit [Å] | 1.799 | 5.380 | 1.800 |
Rmerge | 0.123 | 0.038 | 1.242 |
Rmeas | 0.135 | 0.042 | 1.365 |
Total number of observations | 873618 | ||
Number of reflections | 143089 | 5364 | 22985 |
<I/σ(I)> | 12.36 | 37.4 | 1.32 |
Completeness [%] | 99.8 | 99.9 | 98.7 |
Redundancy | 11.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289 | 0.085 M HEPES, 3.6 M NaCl, 15% Glycerol |