4ZOB
Crystal Structure of beta-glucosidase from Listeria innocua in complex with gluconolactone
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-06-17 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 90.360, 95.810, 213.310 |
Unit cell angles | 90.00, 97.20, 90.00 |
Refinement procedure
Resolution | 41.910 - 2.400 |
R-factor | 0.174 |
Rwork | 0.170 |
R-free | 0.25010 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4zoe |
RMSD bond length | 0.012 |
RMSD bond angle | 1.636 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 41.910 |
High resolution limit [Å] | 2.400 |
Number of reflections | 67092 |
<I/σ(I)> | 6.8 |
Completeness [%] | 100.0 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG 4000, NaCl, LiSO4, glycerol |