4ZLF
Cellobionic acid phosphorylase - cellobionic acid complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-10 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 107.189, 107.189, 186.824 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.140 - 1.600 |
R-factor | 0.15719 |
Rwork | 0.156 |
R-free | 0.17722 |
Structure solution method | SAD |
RMSD bond length | 0.031 |
RMSD bond angle | 2.559 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.411 | |
Number of reflections | 163884 | |
<I/σ(I)> | 37.3 | 2.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.9 | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.1 M sodium citrate, 0.1 M Li2SO4, 0.6 M (NH3)2SO4, 5%(v/v) glycerol |