4ZL9
Crystal structure of Pseudomonas aeruginosa DsbA E82I: Crystal III
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95370 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 35.390, 62.860, 42.090 |
Unit cell angles | 90.00, 98.23, 90.00 |
Refinement procedure
Resolution | 41.657 - 1.700 |
R-factor | 0.1613 |
Rwork | 0.159 |
R-free | 0.20070 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3h93 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.273 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.660 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 19942 | |
<I/σ(I)> | 7.8 | 1.9 |
Completeness [%] | 99.1 | 98.2 |
Redundancy | 3.6 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 20-29 % PEG 1500, 0.1 M MES |