4ZBH
THE CRYSTAL STRUCTURE OF THE SOLUBLE DOMAIN OF SULFOLOBUS ACIDOCALDARIUS FLAF
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 12.3.1 |
Synchrotron site | ALS |
Beamline | 12.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-08-08 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9677 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 52.407, 52.407, 100.241 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.440 - 1.500 |
R-factor | 0.16 |
Rwork | 0.158 |
R-free | 0.19600 |
Structure solution method | SIRAS |
RMSD bond length | 0.005 |
RMSD bond angle | 1.042 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 22800 | |
<I/σ(I)> | 62.6 | 3.7 |
Completeness [%] | 98.4 | 97.6 |
Redundancy | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 288 | 3 M POTASSIUM CHLORIDE AND 50 mM HEPES, PH7.0, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 298K |