4Z7W
T316 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-08-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95370 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 66.623, 200.518, 87.183 |
Unit cell angles | 90.00, 100.63, 90.00 |
Refinement procedure
Resolution | 85.690 - 2.890 |
R-factor | 0.2289 |
Rwork | 0.228 |
R-free | 0.24730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4gg8 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.850 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 85.690 | 3.000 |
High resolution limit [Å] | 2.890 | 2.890 |
Rmerge | 0.117 | 0.421 |
Number of reflections | 45344 | |
<I/σ(I)> | 11.13 | 3.34 |
Completeness [%] | 99.6 | 79.16 |
Redundancy | 4.1 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.32 M (NH4)2SO4, 0.1 M HEPES pH 7.8, 20% PEG3350 |