4YVJ
Crystal Structure of H. influenzae TrmD in complex with sinefungin and tRNA variant (G36U)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-25 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 87.400, 87.400, 229.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.617 - 2.900 |
R-factor | 0.203 |
Rwork | 0.199 |
R-free | 0.27750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4yvi |
RMSD bond length | 0.022 |
RMSD bond angle | 1.593 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.900 |
Number of reflections | 20544 |
<I/σ(I)> | 20 |
Completeness [%] | 99.6 |
Redundancy | 9.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | sodium acetate trihydrate, ammonium phosphate monobasic, PEG 20000 |