4YOP

CRYSTAL STRUCTURE OF HEN EGG-WHITE LYSOZYME

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	FREE ELECTRON LASER
Source details	SACLA BEAMLINE BL3
Synchrotron site	SACLA
Beamline	BL3
Temperature [K]	293
Detector technology	CCD
Collection date	2015-01-30
Detector	MPCCD
Wavelength(s)	1.77
Spacegroup name	P 43 21 2
Unit cell lengths	79.200, 79.200, 37.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.001 - 2.100
R-factor	0.1606
Rwork	0.157
R-free	0.19140
RMSD bond length	0.008
RMSD bond angle	1.074
Phasing software	SHELXDE
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall
Low resolution limit [Å]	40.000
High resolution limit [Å]	2.100
Number of reflections	15532
<I/σ(I)>	24.9
Completeness [%]	100.0
Redundancy	1119

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE	3	293	sodium chloride, PEG 6000