4YNX
Structure of YdiE from E. coli
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2003-03-11 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.900 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.736, 38.189, 54.728 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.500 - 1.500 |
R-factor | 0.175 |
Rwork | 0.171 |
R-free | 0.25020 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | MOLECULAR DYNAMICS SIMULATION OF PDB 2JRA |
RMSD bond length | 0.023 |
RMSD bond angle | 2.028 |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.500 | 1.554 |
High resolution limit [Å] | 1.497 | 1.497 |
Rmerge | 0.063 | 0.346 |
Number of reflections | 12710 | |
<I/σ(I)> | 19.3 | 4.1 |
Completeness [%] | 98.4 | 95.8 |
Redundancy | 4.4 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | 1.6 M ammonium sulphate, 0.1M Tris |