4YEU
ELIC-GLIC chimera in the resting conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-08-24 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979180 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 132.440, 217.960, 229.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 4.600 |
R-factor | 0.2421 |
Rwork | 0.242 |
R-free | 0.24850 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.980 |
Data scaling software | XDS (November 3, 2014) |
Phasing software | PHASER (2.5.6) |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 4.600 |
Number of reflections | 18442 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | PEG 4000, Ammonium Sulfate, Sodium ADA |