4YDZ
Stress-induced protein 1 from Caenorhabditis elegans
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-09-03 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 4 2 2 |
| Unit cell lengths | 142.550, 142.550, 100.580 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 15.000 - 3.600 |
| R-factor | 0.22116 |
| Rwork | 0.220 |
| R-free | 0.23909 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.844 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.700 |
| High resolution limit [Å] | 3.600 | 3.600 |
| Rmerge | 0.082 | 0.523 |
| Number of reflections | 12051 | |
| <I/σ(I)> | 17.6 | 4.4 |
| Completeness [%] | 96.0 | 99 |
| Redundancy | 5.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 100 mM MES, 30% PEG 400, 100 mM NaAc |
