Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-11-16 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 171.370, 538.660, 310.920 |
| Unit cell angles | 90.00, 104.09, 90.00 |
Refinement procedure
| Resolution | 49.099 - 3.000 |
| R-factor | 0.2753 |
| Rwork | 0.274 |
| R-free | 0.30310 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3j32 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.402 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 49.100 |
| High resolution limit [Å] | 3.000 |
| Number of reflections | 1072359 |
| <I/σ(I)> | 7.76 |
| Completeness [%] | 98.9 |
| Redundancy | 2.56 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG400, HEPES, CaCl2 |
